Crystallography Open Database

Information card for entry 7707959

Preview

Coordinates	7707959.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C8 H136 N4 Na14 O214 Se6 W45 Yb4
Calculated formula	C6 H28 N3 Na O181 Se6 W45 Yb4
Title of publication	Assembly of tetra-nuclear Yb<sup>III</sup>-containing selenotungstate clusters: synthesis, structures, and magnetic properties.
Authors of publication	Han, Li-Zhi; Jiao, Cheng-Qi; Chen, Wei-Chao; Shao, Kui-Zhan; Jin, Long-Yi; Su, Zhong-Min
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	33
Pages of publication	11535 - 11541
a	17.1503 ± 0.0013 Å
b	25.5807 ± 0.0019 Å
c	35.868 ± 0.003 Å
α	93.153 ± 0.002°
β	99.868 ± 0.002°
γ	106.34 ± 0.001°
Cell volume	14788 ± 2 Å³
Cell temperature	296.15 K
Ambient diffraction temperature	296.15 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1702
Residual factor for significantly intense reflections	0.0756
Weighted residual factors for significantly intense reflections	0.1707
Weighted residual factors for all reflections included in the refinement	0.2282
Goodness-of-fit parameter for all reflections included in the refinement	1.018
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
268753 (current)	2021-09-06	cif/ Updating files of 7707959, 7707960 Original log message: Adding full bibliography for 7707959--7707960.cif.	7707959.cif
267967	2021-08-06	cif/ Adding structures of 7707959, 7707960 via cif-deposit CGI script.	7707959.cif