Crystallography Open Database

Information card for entry 7707960

Preview

Coordinates	7707960.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H152 N6 Na14 O212 Se6 W44 Yb4
Calculated formula	C8 H36 N4 Na O181 Se6 W44 Yb4
Title of publication	Assembly of tetra-nuclear Yb<sup>III</sup>-containing selenotungstate clusters: synthesis, structures, and magnetic properties.
Authors of publication	Han, Li-Zhi; Jiao, Cheng-Qi; Chen, Wei-Chao; Shao, Kui-Zhan; Jin, Long-Yi; Su, Zhong-Min
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	33
Pages of publication	11535 - 11541
a	50.919 ± 0.002 Å
b	23.3103 ± 0.0008 Å
c	20.2832 ± 0.0008 Å
α	90°
β	90°
γ	90°
Cell volume	24074.9 ± 1.6 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296.15 K
Number of distinct elements	8
Space group number	60
Hermann-Mauguin space group symbol	P b c n
Hall space group symbol	-P 2n 2ab
Residual factor for all reflections	0.119
Residual factor for significantly intense reflections	0.0552
Weighted residual factors for significantly intense reflections	0.112
Weighted residual factors for all reflections included in the refinement	0.1392
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
268753 (current)	2021-09-06	cif/ Updating files of 7707959, 7707960 Original log message: Adding full bibliography for 7707959--7707960.cif.	7707960.cif
267967	2021-08-06	cif/ Adding structures of 7707959, 7707960 via cif-deposit CGI script.	7707960.cif